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Supercritical fluid extraction technology for essential oil extraction of Murraya exotica

By: Muhammad Kaleem Naseem, Muhammad Bilal Chattha, Adnan Younis, Hasan Sardar, Muhammad Asif Hanif, Gulzar Akhtar

Key Words: Absolute oil, Concrete oil, GCMS, Rutaceae, Volatile oil

Int. J. Biosci. 10(4), 151-159, April 2017.

DOI: http://dx.doi.org/10.12692/ijb/10.4.151-159

Abstract

Supercritical fluid extraction (SCFE) is an effective method for extracting the bioactive compounds from planting materials as it is more selective and causes no thermal degradation of components. SCFE gives oil of superior quality because extracts are obtained without using any chemical solvents. Three treatment conditions of temperature and pressure i.e. T1= 35oC/75 bar, T2=40oC/80 bar and T3=45oC/90 bar were employed in this study. Whereas, treatment T2 was found to be superior in getting better yield and quality of essential oil while producing 0.18% concrete oil and 0.008% absolute oil then rest of treatments. Whereas, extraction done at 45oC and 90 bar pressure (T3) gave the second highest concrete (0.17%) and absolute (0.006%) oil yield and T1 (35oC/75 bar) treatment resulted in the lowest concrete (0.15%) and (0.005%) oil yield. Moreover, temperature had more influence on the essential oil extraction of M. exotica through supercritical fluid extraction technique.

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Supercritical fluid extraction technology for essential oil extraction of Murraya exotica

Akram A, Khan MA, Younis A, Ashfaq M. 2014. Exogenous application of 24-epibrassinolide on morpho-physiological, biochemical attributes and essential oil contents of Jasminum sambac L. Pakistan Journal of Agricultural Sciences 51, 881-886.

Anitescu G, Doneanu C, Radulescu V. 1997. Isolation of coriander oil: comparison between steam distillation and supercritical CO2 extraction. Flavour and Fragrance journal 12, 173–176.

Assis LM, Pinto JSS, Lancas FM. 2000. Comparison among different extraction methods (PFE, SFE, Sonication, Soxhlet) for the isolation of organic compounds from coal. Journal of Microcolumn Separations 12, 292-301.

Caredda A, Maringiu B, Porcedda S, Soro C. 2002. Supercritical carbon dioxide extraction and characterization of Laurus nobilis essential oil. Journal of Agricultural and Food Chemistry 50, 1492–1496.

Carlson LHC, Machado RAF, Spricigo CB, Pereira LK, Bolzan A. 2001. Extraction of lemongrass essential oil with dense carbon dioxide. Journal of Supercritical Fluids 21, 33–39.

Diaz-Maroto MC, Perez-Coello MS, Cabezudo MD. 2002. Supercritical carbon dioxide extraction of volatiles from spices, comparison with simultaneous distillation extraction. Journal of Chromatography A 947, 23–34.

Gopalakrishnan N, Shanti PPV, Narayanan CS. 1990. Composition of clove bud oil extracted using carbon dioxide. Journal of the Science of Food and Agriculture 50, 111–117.

Hu Q, Pan B, Xu J, Sheng J, Shi Y. 2007. Effects of supercritical carbon dioxide extraction conditions on yields and antioxidant activity of Chlorella pyrenoidosa extracts. Journal of Food Engineering 80, 997–100.

Joy PP, J. Thomas S, Mathew G, Jose, Joseph J. 2001. Aromatic plants. Tropical Horticulture Vol. 2. (Eds. Bose, T. K., J. Kabir, P. Das and P.P. Joy). Naya Prokash, Calcutta, 633-733 P.

Lang Q, Wai CM. 2001. Supercritical fluid extraction in herbal and natural product studies.Talanta53, 771–782.

Leal PF, Maia NB, Carmello QAC, Catherino RR, Eberlin MNMeireles MA. 2008. Sweet basil (Ocimum basilicum) extracts obtained by supercritical fluid extraction (SFE): Global yields, chemical composition, antioxidant activity and estimation of the cost of manufacturing. Food and Bioprocess Technology 1, 326–338.

Lin MC, Tsai MJ, Wen KC. 1999. Supercritical fluid extraction of flavonoids from Scutellariae Radix. Journal of Chromatography A830, 387–395.

Lis-Balchin M, Deans SG. 1997. Bioactivity of selected plant essential oils against Listeria monocytogenes. Journal of Applied Microbiology 82, 759–762.

LiuS, Yang F, Zhang C, Ji H, Hong P, Deng C. 2009. Optimization of process parameters for supercritical carbon dioxide extraction of Passiflora seed oil by response surface methodology. Journal of Supercritical Fluids 48, 9–14.

Liza  MS, Abdul Rahman R, Mandana B, Jinap S, Rahmat  A, Zaidul ISM. 2009. Supercritical carbon dioxide extraction of bioactive flavonoid from Strobilanthes crispu (Pecah Kaca). Food and Bioproducts Processing 88, 319–326.

Lou V, Folas G, Voutasa E, Magoulas K. 2003. Extraction of parsley seed oil by supercritical CO2. Journal of Supercritical Fluids 7, 1–12.

Mohammed MI, Hamza ZU. 2008. Physicochemical Properties of Oil Extracts from Sesamum indicum L. Seeds Grown in Jigawa State- Nigeria. Journal of Applied sciences and Environmental Management 12(2), 99-101.

Naseem MK, Khan MA, Ahmad R. 2015. Gas chromatography-mass spectrophotometry of Murraya exotica essential oil extracted through different extraction techniques. The Journal of Animal &Plant Sciences 25, 1730-1736.

Nilufer G, Kincala S, Yener E. 2009. Optimization of supercritical carbon dioxide extraction of antioxidant from roasted wheat germ based on yield, total phenolic and tocopherol contents, and antioxidant activities of the extracts. Journal of Supercritical Fluids 48, 217–224.

Omidbaigi R, Sefldkon F, Kazemi F. 2003. Roman chamomile oil: comparison between hydro-distillation and supercritical fluid extraction. Journal of Essential Oil Bearing Plants 6, 191–194.

Paquot C. 1986 a. Spectrophometric  determination of colour. Standard methods for the analysis of oils, fats and derivatives. Centre National de la Recherche Sceintifique, thiais, 2nd Ed, 25-32.

Paquot C. 1986 b. Determination of refractive index, standard methods for the analysis of oils, fats and derivatives. Centre National de la Recherche Sceintifique, thiais, 2″ Ed, 23-24.

Parrotta JA. 2001. Healing plants of Peninsular India. CABI Publishing, Wallingford, UK and New York P, 917.

Reis-Vasco EMC, Coelho JAP, Palavra AMF. 1999. Comparison of pennyroyal oils obtained by supercritical CO2 extraction and hydro-distillation. Flavour and Fragrance Journal 14,156–160.

Reverchon E, Donsi G, Osseo LS. 1993. Modeling of supercritical fluid extraction from herbaceous matrices. Industrial and Engineering Chemistry Research 32, 2721–2726.

Reverchon E. 1997.Supercritical fluid extraction and fractionation of essential oilsandrelated products. Journal of Supercritical Fluids 10, 1-37.

Rezaei K, Temelli F. 2000. Using supercritical fluid chromatography to determine the binary diffusion coefficient of lipids in supercritical CO2. Journal of Supercritical Fluids 17, 35–44.

Sarrazin C, Le Quere JL, Gretsch C, Liardon R. 2000. Representativeness of coffee aroma extracts: a comparison of different extraction methods. Food Chemistry 70, 99- 106.

Steel RGD, Torrie JH, Dickey DA. 1997. Principles and procedures of statistics. A biometrical approach.  McGraw Hill Book International Co., New York, 134-135.

Ueno H, Tanaka M, Machmudah S, Sasaki M, Goto M. 2008. Supercritical carbon dioxide extraction of valuable compounds from Citrus junos seed. Food and Bioprocess Technology 1, 357–363.

Vijayalakshmi A, Tripathi R, Ravichandiran V. 2010. Characterization and evaluation of antidermatophytic of the essential oil from Artimisia nilagirica leaves growing wild in nilgiris. International Journal of Pharmacy and Pharmaceutical Sciences 2, 93-97.

Wang L, Yang B, Du X, Yi C. 2008. Optimization of supercritical fluid extraction of flavonoids from Pueraria lobata. Food Chemistry 108, 737–741.

Wenqiang, G, Li S, Yan R, Tang S, Quan C. 2007. Comparison of essential oils of clove buds extracted with supercritical carbon dioxide and other three traditional extraction methods. Food Chemistry.101, 1558-1564.

Wheeler JR, Mc Nally E. 1989. Separation of palm kernel oil from palm kernel with supercritical carbon dioxide using pressure swing technique. Journal of Chromatographic Science 27, 534–539.

Wood JA, Bernards MA, Wan W, Charpentier PA. 2006. Extraction of ginsenosides From North American ginseng using modified supercritical carbon dioxide. Journal of Supercritical Fluids 39, 40–47.

Younis A, Mehdi A, Riaz A. 2011. Supercritical carbon dioxide extraction and gas chromatography analysis of Jasminum Sambac essential oil. Pakistan Journal of Botany 43, 163-168.

Younis A, Riaz A, Khan MA, Khan AA, Pervez MA. 2008. Extraction and identification of chemical constituents of the essential oil of Rosa species. Acta Horticulturea 766, 485-492.

Younis A, Riaz A, Khan MA, Khan AA. 2007. Effect of different extraction methods on yield and quality of essential oil from four Rosa species. Floriculture Ornamental Biotechnology 1, 73-76.

Younis A, Riaz A, Khan MA, Khan AA. 2009. Effect of time of growing season and time of day for flower harvest on flower yield and essential oil quality and quantity of four Rosa cultivars. Floriculture and Ornamental Biotechnology 3, 98-103.

Muhammad Kaleem Naseem, Muhammad Bilal Chattha, Adnan Younis, Hasan Sardar, Muhammad Asif Hanif, Gulzar Akhtar. 2017. Supercritical fluid extraction technology for essential oil extraction of Murraya exotica. Int. J. Biosci. 10(4), 151-159.
http://dx.doi.org/10.12692/ijb/10.4.151-159
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